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A new method to extract quantitative information from poorly resolved Si magic-angle spinning (MAS) nuclear magnetic resonance (NMR) spectra of natural mixed-layer illite-smectite (I-S) clays29Si i...
Pyrope-grossular solid solutions, (Mg,Ca) Al Si O , of composition Py Gr and Py Gr were3 2 3 12 85 15 75 25 synthesized at 1000, 1200, and 1400 ?C and 30 kbars in a piston-cylinder device. The synt...
Abstract: A swelling mica, Na2Mg3(Al2Si2)O10F2·xH2O, (hereafter “Na-4 mica”) was synthesized from metakaolinite + MgO and Mg aluminosilicate gels at different temperatures and durations using NaF flux...
A magic-angle-spinning nuclear magnetic resonance (MAS NMR) spectroscopic study was done on the series of synthetic gallian-fluor amphiboles to identify the extent of Ga and Si ordering in the Si MA...
29The SiMASNMRspectrumofarmenitefromWasenalp(Valais,Switzerland)indicates completeSi,Alordering.Thesamechemicalshifts(82.3,95.0,and101.8ppm)were alsomeasuredforarmenitefromRe!migny(Quebec,Canada),ho...
We report the compositional systematics of the 29 Si MAS NMR spectra of richterite,[A](Na,K,Rb)1(Na,Ca,Sr)2Mg5Si8O22 (OH,F)2; pargasite, NaCa2Mg4AlSi6Al2O2(OH)2; and fluor-edenite, NaCa2Mg5Si7AlO22F2....
We present 29SiMAS-NMR spectroscopic data for a series of synthetic feldspar samples along the join CaAI2Si20g-SrAI2Si20g, from which the composition dependence and cou- pling of order parameters de...
The structural phase transitions ofmonoclinic tridymite that occur at elevated temper-atures, as wellas the structure of the high-temperature modifications, have been studied by 29SiMASNMR. The sample...
AMonteCarlo method wasdeveloped to determine the distribution ofAland Sications from 29SiMASNMR data for framework aluminosilicates. The method wasused to an-alyze data obtained from Cs-exchanged leuc...
Kaolinite-richsamples wereselectedfor 27 Aland 29SiMASNMRstudy to explore the effectofFeontheir spectraandprovide insight into the nature ofFeorderingin kaolinite. Initial characterization bychemicala...
Examination of two volcanic and two precipitated allophanes by solid-state NMR, thermal analysis and X-ray powder diffraction shows three of the samples to contain structural features similar to both ...
The mechanisms of palygorskite and sepiolite alteration to smectite under mild hydrothermal conditions were investigated by solid-state 27Al and 29Si magic-angle spinning-nuclear magnetic resonance (M...
Solid-state nuclear magnetic resonance (NMR) spectroscopy, thermal analysis, and X-ray powder diffraction data on the tubular, hydrous aluminosilicate imogolite were found to be fully consistent with ...
Abstract: The introduction of artificial ±b/3 stacking faults into well-crystallized kaolinite by intercalating and removing hydrazine had no observable effect on the solid-state 29Si nuclear magnetic...

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